Tetrahydrofuran → HCID 19598372, compound

Participants

Reaction Conditions

Reaction Steps

2.1 ml (15 mmol) of triethylamine in 10 ml of tetrahydrofuran are added dropwise at 25° C. to a solution of 1.5 g (4 mmol) of N-(4-benzyloxycarbonylphenyl)-4-toluenesulfonamide, 1.23 g (4.4 mmol) of acridinecarbonyl chloride hydrochloride and 0.02 g of dimethylaminopyridine in 20 ml of anhydrous tetrahydrofuran. The temperature is raised to 60° C.

Provenance & Evidence