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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 611969Generated: October 31, 2026

Hydrogen Bromide → HCID 19598388, compound

https://huagongshe.com/reaction/611969

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen BromideHCID 260—
ReactantHCID 19598372HCID 19598372—
SolventAcetic AcidHCID 176—
ProductHCID 19598388HCID 19598388—

Reaction Conditions

Temperature60 °C

Reaction Steps

1.17 g (2 mmol) of N-(4-benzyloxycarbonylphenyl)-N-(4-toluenesulfonyl)acridine-9-carboxamide are stirred with 10 ml of 33% strength solution of hydrogen bromide in glacial acetic acid while heating at 60° C. for 4 hours. After cooling, the precipitate is filtered off with suction and dried in vacuo. Yield: 1.00 g (87% of theory)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06002007
Source datasetuspto-grants-1999_12
ORD IDord-6c5b5f1ddc8d44ddbfdc0378f9355def
Source noteuspto-grants-1999_12