HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacryloyl chloride → HCID 10223066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | 6-Amino-4-(3-bromophenylamino)quinoline-3-carbonitrile | HCID 9967712 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 10223066 | HCID 10223066 | 52.8% |
Reaction Steps
Prepared from 0.500 g of 6-amino-4(3-bromophenylamino)quinoline-3-carbonitrile, 0.194 g of Et3N and 0.202 g of methacryloyl chloride in the same manner as Example 380. There was obtained 0.317 g of N-[4-(3-bromophenylamino)-3-cyanoquinolin-6-yl]-2-methylacrylamide as a yellow solid: mass spectrum (electrospray, m/e): M+H 406.8, 408.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06002008 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-eb14928396984da5a03e9767426d8c9d |
| Source note | uspto-grants-1999_12 |