HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromoaniline → HCID 22466660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromoaniline | HCID 11562 | — |
| Reactant | HCID 22466635 | HCID 22466635 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22466660 | HCID 22466660 | — |
Reaction Steps
Prepared from 0.400 g of 4-chloro-6-dimethylaminoquinoline-3-carbonitrile and 3-bromoaniline in the same manner as Example 377. The crude product was boiled twice with EtOAc and dried in vacuo (50° C.). The yield of 4(3-bromophenylamino)-6-dimethylaminoquinoline-3-carbonitrile hydrochloride was 0.621 g as a brown powder: mass spectrum (electrospray, m/e) M+H 366, 368.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06002008 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-265c42fdcba44f609cd9daf6db932524 |
| Source note | uspto-grants-1999_12 |