HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1,1,1-trifluoroethane → HCID 178447772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1,1,1-trifluoroethane | HCID 67898 | — |
| Reactant | 4-(t-Butyldimethylsiloxy)benzyltriphenylphosphonium bromide | HCID 10393091 | — |
| Reactant | 4-(4-Phenyl-4-n-pentyl-4-silacyclohexyl)cyclohexane carbaldehyde | HCID 53863304 | — |
| Product | HCID 178447772 | HCID 178447772 | — |
Reaction Steps
The general procedure of Example 38 was repeated using 4-(t-butyldimethylsiloxy)benzyltriphenylphosphonium bromide, 4-(4-n-pentyl-4-phenyl-4-silacyclohexyl)cyclohexane carbaldehyde, and 1-bromo-2,2,2-trifluoroethane, thereby obtaining the intended compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06004478 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-1e24cbf6d84b40219cfec86ed087f688 |
| Source note | uspto-grants-1999_12 |