HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 19595374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178441902 | HCID 178441902 | — |
| Product | HCID 19595374 | HCID 19595374 | — |
Reaction Steps
Using the procedure of Step F of Example 1, 1.2 g of the product of Step B and 10 ml of phosphorous oxychloride were reacted to obtain after chromatography on silica (eluant: hexane-ethyl acetate (6.4)), 1.16 g of the desired product melting at <50° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06004979 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-32e1b03ea4fe4eb083d476044786d33f |
| Source note | uspto-grants-1999_12 |