HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23283700, compound → HCID 23283705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23283700 | HCID 23283700 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23283705 | HCID 23283705 | — |
Reaction Steps
The product N-[2-(1-carbethoxy-2-acetyl-5-methoxyindol-3-yl)ethyl]acetamide (100 mg) is dissolved in ethanol (10 ml) in a round-bottomed flask (25 ml), 100 mg of Pd(OH)2 are added and the mixture is stirred for 12 h at a normal pressure of hydrogen. After filtration, N-[2-(1-carbethoxy-2-acetyl-5-methoxyindolin-3-yl)-ethyl]acetamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06004991 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-2674648fe9124453b5af7ce91411fdcb |
| Source note | uspto-grants-1999_12 |