HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Dimethyl 4-(4-methoxybenzyloxy)phthalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Reactant | Dimethyl 4-hydroxyphthalate | HCID 89726 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Dimethyl 4-(4-methoxybenzyloxy)phthalate | HCID 19595683 | — |
Reaction Steps
1 eq. of dimethyl 4-hydroxyphthalate, 1.1 eq. of potassium carbonate and 1.1 eq. of 4-methoxybenzyl chloride were stirred in DMF at RT. After 4 days, the mixture was worked up according to a standard procedure. Dimethyl 4-(4-methoxybenzyloxy)phthalate was isolated as a colorless oil. MS: 331 ((M+1)+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005010 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-6aa64a686a13461fbdec1ab546ad0f32 |
| Source note | uspto-grants-1999_12 |