HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 54436784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | N-Acetylsulfanilyl chloride | HCID 8481 | — |
| Product | HCID 54436784 | HCID 54436784 | — |
Reaction Steps
The sulfonamide was synthesized from 4-acetamidophenyl sulfonyl chloride (0.01 mol) and o-phenylene diamine (0.01 mmol) by general Method C. It was purified by recrystallization from EtOH (1.27 g, 40%) EI-MS m/z 304 (M-H)-.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005008 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-3e586d5f1da148ebac9d0abc7b623efd |
| Source note | uspto-grants-1999_12 |