HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenyl isocyanate → HCID 22011327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | HCID 54436784 | HCID 54436784 | — |
| Product | HCID 22011327 | HCID 22011327 | 24% |
Reaction Steps
The urea was synthesized from 2-[(4-acetamidophenyl)sulfonylamino]phenyl aniline (1 mmol) and 2-bromo phenyl isocyanate (1 mmol) by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane. Filtering afforded the desired compound (0.12 g, 24%). EI-MS m/z 50 (M-H)-
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005008 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-ef09405481f5410fa940d57014755b46 |
| Source note | uspto-grants-1999_12 |