HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenyl isocyanate → N-(2-(benzylsulfonylamino)phenyl) N'-(2-bromophenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | 2-(Benzylsulfonylamino)aniline | HCID 16778443 | — |
| Product | N-(2-(benzylsulfonylamino)phenyl) N'-(2-bromophenyl)urea | HCID 54425527 | 23.9% |
Reaction Steps
The urea was synthesized from 2-(benzyl sulfonyl amino) aniline (1 mmol) and 2-bromo phenyl isocyanate (1 mmol) by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane. Filtering afforded the desired compound (0.11 g, 23%). EI-MS m/z 460 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005008 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-e2f7a9de0eab4a3193ecb260535f769d |
| Source note | uspto-grants-1999_12 |