HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenyl isocyanate → HCID 53805601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | HCID 3476927 | HCID 3476927 | — |
| Product | HCID 53805601 | HCID 53805601 | — |
Reaction Steps
The title compound was prepared from [2-(3,5-bistrifluoromethylphenyl) sulfonylaminoaniline (591 mg, 1.5 mmol) and 2-bromophenylisocyanate (305 mg, 1.5 mmol) according to General Method B. The product was purified by flash chromatography on silica gel (ethyl acetate:hexane 30/70) (10 mg, 1%). EI-MS m/z 580 (M-H)-
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005008 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-f11794ab7f1d48cda8ef5b23798ea023 |
| Source note | uspto-grants-1999_12 |