Cyclopentylamine → HCID 67559013, compound

HRID 612722Notes

Reaction equation

HRID 612722 reaction equation
Cl[S:2][C:3]1C=CC=C[C:4]=1[C:5](Cl)=[O:6].[CH:12]1([NH2:17])[CH2:16][CH2:15][CH2:14][CH2:13]1>>[CH:12]1([N:17]2[C:5](=[O:6])[CH2:4][CH2:3][S:2]2)[CH2:16][CH2:15][CH2:14][CH2:13]1

Participants

3

Reactant 2

HCID 2906CyclopentylamineHCID 109107152-(Chlorothio)-benzoyl chloride

Product 1

HCID 67559013HCID 67559013, compound

Procedure

This was prepared in analogous manner to that described in Example 17 except using 2-chlorosulphenylbenzoyl chloride (5.175 parts, 0.025M) and cyclopentylamine (8.52 parts, 0.1M ex Aldrich). The product was obtained as a yellow oil (5.9 parts) which was recrystallised form hexane mp 87-88° C.

Workup

  1. customThis was prepared in analogous manner to that
  2. customThe product was obtained as a yellow oil (5.9 parts) which
  3. customwas recrystallised form hexane mp 87-88° C.

Sources & evidence

ORD record
ord-cd7e46cb3de944249bea85bf2a54112b
Source dataset
uspto-grants-1999_12
Patent number
US06005032

Reaction notes

Loading…