Isobutylamine → HCID 21099553, compound

HRID 612723Notes

Reaction equation

HRID 612723 reaction equation
Cl[S:2][C:3]1[CH:11]=[CH:10][CH:9]=[CH:8][C:4]=1[C:5](Cl)=[O:6].[CH2:12]([NH2:16])[CH:13]([CH3:15])[CH3:14]>>[CH3:14][CH:13]([CH3:15])[CH2:12][N:16]1[C:5](=[O:6])[C:4]2[CH:8]=[CH:9][CH:10]=[CH:11][C:3]=2[S:2]1

Participants

3

Reactant 2

HCID 6558IsobutylamineHCID 109107152-(Chlorothio)-benzoyl chloride

Product 1

HCID 21099553HCID 21099553, compound

Procedure

This was prepared by the process described in Example 17 except using 2-chlorosulphenylbenzoyl chloride (4.14 parts, 0.02M) and isobutylamine (7.95 parts, 0.08M). The product (4 parts, 97% theory) was obtained as a pale yellow oil.

Workup

  1. customThis was prepared by the process
  2. customThe product (4 parts, 97% theory) was obtained as a pale yellow oil

Sources & evidence

ORD record
ord-dc93bd8865504f0490ceef895ef5c1e4
Source dataset
uspto-grants-1999_12
Patent number
US06005032

Reaction notes

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