HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19595667, compound → HCID 53989278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19595667 | HCID 19595667 | — |
| Reactant | HCID 86754974 | HCID 86754974 | — |
| Product | HCID 53989278 | HCID 53989278 | 97% |
Reaction Steps
The above cyclopropyl aldehyde 10 (29 mg, 0.13 mmol) and 3-ethoxycarbonyl-2-methylprop-2-enylphosphonate (215 mg, 0.82 mmol) were condensed as described for Example 1 to give 33 mg of ethyl-6-[1-(3,5-di-t-butyl phenyl)-cyclopropyl]-3-methyl-2,4-hexadienoate (11) as a pale yellow oil in 97% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005007 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-fd3253936a8843da9b4bb5b420818a30 |
| Source note | uspto-grants-1999_12 |