HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19595667, compound → HCID 53989278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19595667 | HCID 19595667 | — |
| Reactant | HCID 86754974 | HCID 86754974 | — |
| Product | HCID 53989278 | HCID 53989278 | 91% |
Reaction Steps
The above cyclopropyl aldehyde 10 (520 mg, 2.4 mmol) and 3-ethoxycarbonyl-2-methylprop-2-enylphosphonate (2.53 g, 9.6 mmol) were condensed as described for Example 1 to give 712 mg of ethyl-6-[1-(3,4-diethylbenzene)-cyclopropyl]-3-methyl-2,4-hexadienoate (11) as a pale yellow oil in 91% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005007 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-bfa59bec26404e2a8289a869bc3c2d5f |
| Source note | uspto-grants-1999_12 |