HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → Cyclohexanamine, N-[(2-methoxyphenyl)methylene]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Product | Cyclohexanamine, N-[(2-methoxyphenyl)methylene]- | HCID 10775151 | — |
Reaction Steps
A solution of anisaldehyde (21 g) and cyclohexylamine (15 g) in chloroform. (100 ml) was stirred at room temperature for 2 hours and evaporated to afford brown syrup (35 g, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06004989 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-293bf69142cc491f86def577d4567291 |
| Source note | uspto-grants-1999_12 |