HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-amino-2-(((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)amino)benzoate → HCID 15654678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-amino-2-(((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)amino)benzoate | HCID 15654653 | — |
| Reactant | HCID 86584013 | HCID 86584013 | — |
| Product | HCID 15654678 | HCID 15654678 | 25% |
Reaction Steps
The title compound was prepared as pale yellow crystals from methyl 3-amino-2-[[(2'-cyanobiphenyl-4-yl)methyl]amino]benzoate and 2,2,2-trifluoroethyl orthocarbonate according to the procedure for Working Example 3. Yield: 25%, m.p. 143-145° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06004989 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-9598c0f51bbe40bf8f08641652eb6b27 |
| Source note | uspto-grants-1999_12 |