HRID612857

反应详情

EQUATION

反应方程式

HRID 612857 的结构方程式

PROCEDURE

实验过程

A solution of 4N hydrochloric acid/1,4-dioxane (4.0 ml) was added to 3-(2-(N-tert-butoxycarbonylamino)ethoxy)-5-phenylisoxazole (0.50 g), and the mixture was stirred at room temperature for 15 minutes. The precipitate was separated from the mixture by filtration and washed with ethyl acetate to obtain the title compound (0.39 g, 99%) as colorless crystals.

WORKUP

后处理

  1. customThe precipitate was separated from the mixture by filtration
  2. washwashed with ethyl acetate