HRID612857
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
A solution of 4N hydrochloric acid/1,4-dioxane (4.0 ml) was added to 3-(2-(N-tert-butoxycarbonylamino)ethoxy)-5-phenylisoxazole (0.50 g), and the mixture was stirred at room temperature for 15 minutes. The precipitate was separated from the mixture by filtration and washed with ethyl acetate to obtain the title compound (0.39 g, 99%) as colorless crystals.
WORKUP
后处理
- customThe precipitate was separated from the mixture by filtration
- washwashed with ethyl acetate