HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → 3-(2-(N-tert-Butoxycarbonylamino)ethoxy)-5-phenyl-4-propylisoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 3-(2-(N-tert-butoxycarbonylamino)ethoxy)-5-phenylisoxazole | HCID 15434960 | — |
| Product | 3-(2-(N-tert-Butoxycarbonylamino)ethoxy)-5-phenyl-4-propylisoxazole | HCID 19596718 | 65% |
Reaction Steps
3-(2-(N-tert-Butoxycarbonylamino)ethoxy)-5-phenylisoxazole (0.3 g) and propyl iodide (0.29 ml) were subjected to reaction and post-treatment in a similar manner to that described in Example 14(a) to obtain the title compound (0.22 g, 65%) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005116 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-e3a6a69b7b634e9483b441f8f1102e85 |
| Source note | uspto-grants-1999_12 |