HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbutanal → HCID 19596637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbutanal | HCID 11552 | — |
| Reactant | 3-(2-(N-tert-butoxycarbonylamino)ethoxy)-5-phenylisoxazole | HCID 15434960 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 19596637 | HCID 19596637 | 77% |
Reaction Steps
3-(2-(N-tert-Butoxycarbonylamino)ethoxy)-5-phenylisoxazole (0.2 g), butyllithium (1.6M hexane solution, 0.9 ml) and isovaleraldehyde (0.09 ml) were subjected to reaction and post-treatment in a similar manner to that described in Example 44(a) to obtain the title compound (0.2 g, 77%) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005116 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-4132f9e6504a44ddbbb78e7fc7149392 |
| Source note | uspto-grants-1999_12 |