Ethanol → HCID 54312806, compound

HRID 612948Notes

Reaction equation

HRID 612948 reaction equation
[F:1][C:2]([F:15])([F:14])[C:3]1[CH:13]=[CH:12][CH:11]=[CH:10][C:4]=1[CH:5]=[CH:6][C:7]([OH:9])=[O:8].S(=O)(=O)(O)O.[CH2:21](O)[CH3:22]>>[CH2:21]([O:8][C:7](=[O:9])[CH:6]=[CH:5][C:4]1[CH:10]=[CH:11][CH:12]=[CH:13][C:3]=1[C:2]([F:14])([F:15])[F:1])[CH3:22]

Participants

4

Reactant 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 749393-(2-(Trifluoromethyl)phenyl)-2-propenoic acid

Product 1

HCID 54312806HCID 54312806, compoundYield 95%

Procedure

2-Trifluoromethylcinnamic acid (10.1 g), conc. sulfuric acid (1 ml) and ethanol (100 ml) were subjected to reaction and post-treatment in a similar manner to that described in Reference example 10(a) to obtain the title compound (10.8 g, 95%) as a colorless oil.

Sources & evidence

ORD record
ord-0df1bdf92f0941e398042b0928e42867
Source dataset
uspto-grants-1999_12
Patent number
US06005116

Reaction notes

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