HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 3-[4-(trifluoromethyl)phenyl]prop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-[4-(Trifluoromethyl)phenyl]prop-2-enoic acid | HCID 74940 | — |
| Product | Ethyl 3-[4-(trifluoromethyl)phenyl]prop-2-enoate | HCID 53662772 | 95% |
Reaction Steps
4-Trifluoromethylcinnamic acid (10.2 g), conc. sulfuric acid (1 ml) and ethanol (100 ml) were subjected to reaction and post-treatment in a similar manner to that described in Reference example 10(a) to obtain the title compound (10.9 g, 95%) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005116 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-647153e9d1d844f2812bd8057db26733 |
| Source note | uspto-grants-1999_12 |