Ethanol → HCID 11264629, compound

HRID 612958Notes

Reaction equation

[C:1]1([C:11](=[CH2:15])[C:12]([OH:14])=[O:13])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.S(=O)(=O)(O)O.[CH2:21](O)[CH3:22]>>[CH2:21]([O:13][C:12](=[O:14])[C:11]([C:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1)=[CH2:15])[CH3:22]

Participants

Reactant 3

HCID 702Ethanol

HCID 1118Sulfuric Acid

HCID 240501NSC46721

Product 1

HCID 11264629HCID 11264629, compoundYield 94%

Procedure

1-Naphthylacrylic acid (9.5 g), conc. sulfuric acid (1 ml) and ethanol (100 ml) were subjected to reaction and post-treatment in a similar manner to that described in Reference example 10(a) to obtain the title compound (10.2 g, 94%) as a colorless oil.

Sources & evidence

ORD record: ord-29fd3b5174fc4327a949bffebbcbd500
Source dataset: uspto-grants-1999_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06005116

Reaction notes

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