Ethyl isovalerate → HCID 54415652, compound

HRID 612961Notes

Reaction equation

HRID 612961 reaction equation
[F:1][C:2]1[CH:10]=[C:9]([F:11])[CH:8]=[CH:7][C:3]=1[C:4](Cl)=[O:5].[CH2:12]([O:14][C:15](=[O:20])[CH2:16][CH:17]([CH3:19])[CH3:18])[CH3:13]>>[CH2:12]([O:14][C:15](=[O:20])[CH:16]([C:4](=[O:5])[C:3]1[CH:7]=[CH:8][C:9]([F:11])=[CH:10][C:2]=1[F:1])[CH:17]([CH3:19])[CH3:18])[CH3:13]

Participants

3

Reactant 2

HCID 7945Ethyl isovalerateHCID 5880812,4-Difluorobenzoyl chloride

Product 1

HCID 54415652HCID 54415652, compoundYield 68%

Procedure

2,4-Difluorobenzoyl chloride (4.9 ml) and isovaleric acid ethyl ester (3.0 ml) were subjected to reaction and post-treatment in a similar manner to that described in Reference example 8(a) to obtain the title compound (3.65 g, 68%) as a colorless liquid.

Sources & evidence

ORD record
ord-d13012d78fb24c3b8680a3c3ca90795c
Source dataset
uspto-grants-1999_12
Patent number
US06005116

Reaction notes

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