HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 54713212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Cyclohexanethiol | HCID 15290 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | HCID 54681365 | HCID 54681365 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 54713212 | HCID 54713212 | — |
Reaction Steps
The title compound was prepared by Method C using 4-hydroxy-6-[3-methyl-4-(3-pyridinylmethoxy)phenyl]-2H-pyran-2-one (0.5 g, 1.62 mmol), benzaldehyde (0.189 g, 1.78 mmol), cyclohexylmercaptan (0.489 g, 4.212 mmol), piperidine, (0.5 mL), acetic acid (0.5 mL). m.p. 84-87° C. (d); IR (KBr) 3059, 2930, 2853, 1676, 1601, 1449, 1260, 1134, 700 cm-1 ; MS (CI) m/e 446 (2), 331 (9), 226 (61), 205 (24), 135 (44).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005103 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-f371cf55601f4c2c8c3c2cd44969b18c |
| Source note | uspto-grants-1999_12 |