HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,6-Dimethylpyridin-4-yl)ethan-1-one → HCID 54681250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,6-Dimethylpyridin-4-yl)ethan-1-one | HCID 13227323 | — |
| Reactant | [(Phenylmethyl)thio]propanedioic acid | HCID 19596125 | — |
| Product | HCID 54681250 | HCID 54681250 | — |
Reaction Steps
The title compound was prepared from the condensation of the trimethylsilyl enol ether of 4-acetyl-2,6-dimethylpyridine and the diethyl ester of [(phenylmethyl)thio]propanedioic acid following the same procedure outlined in Method A; m.p. 88-90° C. NMR (DMSO-d6) δ2.55 (s, 6 H), 4.02 (s, 2 H), 6.85 (s, 1 H), 7.16-7.28 (m, 5 H), 7.40 (s, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06005103 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-2ce1f0d4978e4a8295d40754849c7180 |
| Source note | uspto-grants-1999_12 |