[1-(1,2-Dimethyl-propyl)-4-methyl-cyclohex-3-enyl]-methanol → 4-(1,2-Dimethyl-propyl)-1-methyl-2-oxa-bicyclo[2.2.2]octane

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

[1-(1,2-Dimethyl-propyl)-4-methyl-cyclohex-3-enyl]-methanol (268 g, obtained as detailed above), MSA (10 g), and toluene (300 mL) were charged to a 2 L reaction flask, heated to 60° C., and aged for 12 hours. The reaction mixture was cooled, washed with saturated sodium carbonate solution, and distilled to provide 4-(1,2-dimethyl-propyl)-1-methyl-2-oxa-bicyclo[2.2.2]octane (146 g).

Herkunft & Nachweise