HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichlorobenzene → HCID 22459170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichlorobenzene | HCID 7239 | — |
| Reactant | 4-(4'-Methylphenoxy)phenyl allyl ether | HCID 22458892 | — |
| Product | HCID 22459170 | HCID 22459170 | — |
Reaction Steps
4-(4'-Methylphenoxy)phenyl allyl ether (4.00 g, 16.37 mmol) was taken up in 1,2-dichlorobenzene (50 mL) and refluxed for 20 h. After cooling, the solvent was removed in vacuo and the resulting crude oil was chromatographed on silica gel (15% ethyl acetate/hexane) to afford 4-(4'-methylphenoxy)-2-allylphenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06008237 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-44bed392c67a4da18bea343918911cd6 |
| Source note | uspto-grants-1999_12 |