HCID 19592378, compound → HCID 19592998, compound

Participants

Reaction Steps

To a solution of 8-(2,6-dichlorobenzoylamino)-3-(1-hydroxyethyl)quinoline (562 mg) in dichloromethane (20 ml) was added manganese (IV) oxide (2.71 g), and the mixture was stirred at ambient temperature overnight. Insoluble material was filtered off, and the filtrate was concentrated in vacuo. The residue was crystallized from ethanol to give 3-acetyl-8-(2,6-dichlorobenzoylamino)quinoline (101 mg).

Provenance & Evidence