Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 4-Chloro-8-(2,6-dichlorobenzoylamino)quinoline | HCID 19592564 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19592600 | HCID 19592600 | 83.4% |
Reaction Steps
To a solution of 4-chloro-8-(2,6-dichlorobenzoylamino)quinoline (659 mg) in dimethyl sulfoxide (10 ml) was added sodium azide (487 mg), and the mixture was stirred at 90° C. for 8 hours. The mixture was diluted with water (20 ml), and the precipitate was filtered and washed with water to give 4-azido-8-(2,6-dichlorobenzoylamino)quinoline (560 mg) as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06008230 |
|---|
| Source dataset | uspto-grants-1999_12 |
|---|
| ORD ID | ord-da92863de3334e0896c98595ba95dac9 |
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| Source note | uspto-grants-1999_12 |
|---|
