Triphenylphosphine → 8-(2,6-Dichlorobenzoylamino)-4-[(triphenylphosphoranylidene)amino]quinoline

Participants

Reaction Conditions

Reaction Steps

To a suspension of 4-azido-8-(2,6-dichlorobenzoylamino)quinoline (518 mg) in ethyl acetate (5 ml) was added triphenylphosphine (383 mg), and the mixture was stirred for 3 hours at 45° C. The resulting precipitates were collected by filtration, and the residue was recrystallized from ethanol to give 8-(2,6-dichlorobenzoylamino)-4-[(triphenylphosphoranylidene)amino]quinoline (846 mg) as white crystal.

Provenance & Evidence