HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-4-nitrobenzyl alcohol → (4-Amino-3-methoxyphenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-4-nitrobenzyl alcohol | HCID 602961 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (4-Amino-3-methoxyphenyl)methanol | HCID 53420748 | 108.8% |
Reaction Steps
A mixture of 3-methoxy-4-nitrobenzyl alcohol (1.0 g) and 10% palladium on carbon (100 mg) in methanol was stirred for 2 hours under 3 atmospheric pressure of hydrogen. After filtration, the filtrate was concentrated in vacuo to give 4-amino-3-methoxybenzyl alcohol (910 mg) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06008229 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-91bce1332ac54aae9e0c19f0f9b55334 |
| Source note | uspto-grants-1999_12 |