HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 3-(chlorosulfonyl)propanoate → Methyl 3-[2-[2-(4-methylphenyl)ethoxy]ethylaminosulphonyl]propanoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 3-(chlorosulfonyl)propanoate | HCID 4962888 | — |
| Edukt | 2-[2-(4-Methylphenyl)ethoxy]ethanamine hydrochloride | HCID 18779075 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Methyl 3-[2-[2-(4-methylphenyl)ethoxy]ethylaminosulphonyl]propanoate | HCID 18779034 | 46,6% |
Reaktionsschritte
The subtitle compound (2.49 g) was prepared according to the procedure in example 5 part d using 2-[2-(4-methylphenyl)ethoxy]ethanamine hydrochloride (3.5 g) triethylamine 4.74 ml) methyl 3-(chlorosulphonyl)propanoate (3.08 g), and dichloromethane (80 ml).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06008365 |
| Quelldatensatz | uspto-grants-1999_12 |
| ORD ID | ord-0ec0131e5d904d679d7cc6af6447f5ea |
| Quellennotiz | uspto-grants-1999_12 |