HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron Trichloride → Boron Trichloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron Trichloride | HCID 25135 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | Diboron | HCID 6328200 | — |
| Product | Boron Trichloride | HCID 25135 | — |
| Product | HCID 16217148 | HCID 16217148 | — |
Reaction Steps
BCl3 was prepared by passing BCl3 gas slowly into dioxane at 0° C. The adduct thus obtained is a solid which melts at 56° C. (with decomposition), but is stable at 0° C. for several weeks. Reaction of this adduct with diborane in dioxane produces dioxane-BH2Cl as outlined in the following equation. ##STR1##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06008414 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-7d13df6b427545efa3b3350d4f05d134 |
| Source note | uspto-grants-1999_12 |