참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydroquinone | HCID 785 | — |
| 반응물 | Dimethyl Ether | HCID 8254 | — |
| 반응물 | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| 반응물 | Sulphobenzoic anhydride | HCID 13795534 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Methacryloxyethyl sulfobenzoate | HCID 23594379 | — |
반응 단계
Hydroxyethyl methacrylate (65 g.), o-sulfobenzoic anhydride (92 g.), the monomethyl ether of hydroquinone (0.2 g.) and toluene (157 g.) are stirred, sparged with dry air, and heated at 110° C. for 2 hours and then cooled to room temperature. Analysis indicates an approximately 74% conversion of anhydride into methacryloxyethyl sulfobenzoate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04143020 |
|---|
| 출처 데이터셋 | uspto-grants-1979_03 |
|---|
| ORD ID | ord-f17de0b25dda40268fdaec01d9c5f6cb |
|---|
| 출처 메모 | uspto-grants-1979_03 |
|---|
