HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N-Dimethyltetradecylamine → HCID 86733511, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N-Dimethyltetradecylamine | HCID 8211 | — |
| Edukt | Bromomethyl tricyclo[3.3.1.13,7]dec-1-yl ketone | HCID 197820 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | HCID 86733511 | HCID 86733511 | 84,2% |
Reaktionsschritte
A mixture of 1.3g. (0.005 mole) 1-adamantyl bromomethyl ketone and 1.23g (0.005 mole) dimethyltetradecylamine was solubilized by the addition of 30cc acetone. The next day the solidified mixture was washed with ether and recrystallized from ethyl acetate to yield 2.1g white crystals, m.p. 134°-135.5°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04143127 |
| Quelldatensatz | uspto-grants-1979_03 |
| ORD ID | ord-7f8144f1ac4a41dd89582865bff2707e |
| Quellennotiz | uspto-grants-1979_03 |