HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bromide → HCID 178431947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | 2-(2-[Aminomethyl]phenylthio)acetic acid | HCID 20381575 | — |
| Reactant | HCID 178431949 | HCID 178431949 | — |
| Product | HCID 178431947 | HCID 178431947 | 14% |
Reaction Steps
The title compound is prepared in 14% yield, as a colorless amorphous solid, by acylation of 6-amino-2,2-dimethyl-3-(5-tetrazolyl)penam with 2-(2-[aminomethyl]phenylthio)acetic acid (U.S. Pat. No. 3,766,176), using the method of Example LXXVII. IR(KBr disc): 1780 and 1665 cm-1. NMR (DMSO-d6 /D2O): 7.50 ppm (m, 4H), 5.70 ppm (d, 1H), 5.43 ppm (d, 1H), 5.19 ppm (s, 1H), 4.35 ppm (s, 2H), 3.94 ppm (s, 2H), 1.60 ppm (s, 3H), and 1.00 ppm (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04143039 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-ccdea87ed5064b6582af1ca281db8aa9 |
| Source note | uspto-grants-1979_03 |