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HRID614290

反应详情

EQUATION

反应方程式

HRID 614290 的结构方程式

REACTANTS

反应物

2
结构：[Na+].[Na+].[Na+].[O-]P([O-])([O-])=S
HCID9877537

Trisodium thiophosphate

Na3O3PS

结构：Cl.N=C(CCl)NC1Cc2ccccc2C1
HCID178479214

未命名化合物

PRODUCTS

生成物

1
结构：Cl.N=C(CS)NC1Cc2ccccc2C1
HCID178479245

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The procedures described above in Example 1 were carried out on 4.0 g. (0.0149 mole) of the product of Step A above and 2.68 g. (0.0149mole) of trisodiumphosphorothioate in 25 ml. of water. The product was recrystallized from ethanol: ether [m.p. 102-103° C. (decomposition)].

WORKUP

后处理

  1. customThe product was recrystallized from ethanol