Trisodium thiophosphate → HCID 178479245, compound

HRID 614290Notes

Reaction equation

HRID 614290 reaction equation
Cl.[Cl:2][CH2:3][C:4]([NH:6][CH:7]1[CH2:15][C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH2:8]1)=[NH:5].P(=[S:20])([O-])([O-])[O-].[Na+].[Na+].[Na+]>O>[ClH:2].[CH2:8]1[C:9]2[C:14](=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH2:15][CH:7]1[NH:6][C:4](=[NH:5])[CH2:3][SH:20]

Participants

4

Reactant 2

HCID 9877537Trisodium thiophosphateHCID 178479214HCID 178479214, compound

Product 1

HCID 178479245HCID 178479245, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The procedures described above in Example 1 were carried out on 4.0 g. (0.0149 mole) of the product of Step A above and 2.68 g. (0.0149mole) of trisodiumphosphorothioate in 25 ml. of water. The product was recrystallized from ethanol: ether [m.p. 102-103° C. (decomposition)].

Workup

  1. customThe product was recrystallized from ethanol

Sources & evidence

ORD record
ord-ad4528075d15412282c9ea1b8d0614a3
Source dataset
uspto-grants-1979_03
Patent number
US04144271

Reaction notes

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