Allyl bromide → HCID 21329312, compound

Participants

Reaction Steps

Treat a suspension of 1.4 g. (0.005 mole) of the imidazopyridine product of Step D in 80 ml. of acetone with 560 mg. (0.01 mole) of powdered potassium hydroxide. Stir at room temperature for 20 minutes and add 1.21 g. (0.01 mole) of allyl bromide. Continue stirring overnight. Concentrate the reaction mixture to one-half volume and dilute with 75 ml. of water. Separate the solid product by filtration and crystalize from ethanol.

Provenance & Evidence