HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 21329388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | HCID 13346862 | HCID 13346862 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21329388 | HCID 21329388 | — |
Reaction Steps
A mixture of 7.2g (0.05 mole) of 1-thiacyclooctane-5-one and 6.0g (0.056 mole) of phenylhydrazine in 40 ml of glacial acetic acid is refluxed for three hours under nitrogen. On standing there is deposited 5.2g of a solid, m.p. 106°-107° C. Recrystallization from cyclohexane affords 4.9g (45%) of an analytical sample m.p. 109°-110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144349 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-6a4b55a40b8c4163ba5428d9d77c5d98 |
| Source note | uspto-grants-1979_03 |