2-Chloro-N,N-dimethylethylamine → HCID 21329389, compound

Participants

Reaction Steps

A mixture of 12.47g (0.05 mole) of 1,2,4,5,6,7-hexahydrothiocino[5,4-b]indole 3,3-dioxide, 2.1g (0.05 mole) of 57% dispersion sodium hydride and 5.44g (0.05 mole) of 2-dimethylaminoethyl chloride is treated according to the procedure in Example 6. There is deposited 15.3g (96%) of a solid, m.p. 154°-155° C. Recrystallization from ethyl acetate gives 11.2g (70%) of an analytical sample, m.p. 155°-156° C.

Provenance & Evidence