HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 2,5-Di(acetoxymethyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-methyl-5-acetoxymethylpyridine-N-oxide | HCID 20263970 | — |
| Product | 2,5-Di(acetoxymethyl)pyridine | HCID 20263986 | — |
Reaction Steps
2-Methyl-5-acetoxymethylpyridine-N-oxide (0.05 mole) is refluxed in 50 ml. of acetic anhydride for two hours and then evaporated to dryness. The residue is fractionally distilled under high vacuum to obtain 2,5-di(acetoxymethyl)pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04144342 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-b8d4693ba77545a8b0e92e4c8c98152d |
| Source note | uspto-grants-1979_03 |