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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 614529Generated: October 30, 2026

Acetyl chloride → HCID 12909300, compound

https://huagongshe.com/reaction/614529

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetyl chlorideHCID 6367—
ReactantHCID 12909299HCID 12909299—
SolventDimethylformamideHCID 6228—
ProductHCID 12909300HCID 1290930072%

Reaction Steps

By the procedure of Step C in Example 1, methyl 8-amino-4H-imidazo[2,1-c][1,4]-benzoxazine-2-carboxylate and acetyl chloride were reacted in dimethylformamide as solvent to obtain a 72% yield of methyl 8-acetamido-4H-imidazo-[2,1-c][1,4]-benzoxazine-2-carboxylate with a melting point of 216-9° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04145419
Source datasetuspto-grants-1979_03
ORD IDord-e2c29dd5f5be4a5285dddd60dcbcae33
Source noteuspto-grants-1979_03