HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Oxide → Ethanol, 2-[(2,2,6,6-tetramethyl-4-piperidinyl)amino]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Oxide | HCID 6354 | — |
| Reactant | 4-Amino-2,2,6,6-tetramethylpiperidine | HCID 37524 | — |
| Product | Ethanol, 2-[(2,2,6,6-tetramethyl-4-piperidinyl)amino]- | HCID 10703227 | — |
Reaction Steps
156 parts of 4-amino-2,2,6,6-tetramethylpiperidine were heated to 150° C. and ethylene oxide was introduced until 44 parts thereof had been taken up. After fractional distillation, there were obtained 111 parts of 4-(β-hydroxy-ethyl)amino-2,2,6,6-tetramethylpiperidine boiling at 125° C./0.1 torr (melting point 89° to 91° C.) as well as compound 4) as higher boiling fraction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04145512 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-7c8860c6a30e4e2da51d2ba8ff41b04e |
| Source note | uspto-grants-1979_03 |