Dimethylazanide → HCID 22749551, compound

HRID 614713Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]3[CH:12]=[N:13][C:14]([C:15]([O:17]C)=O)=[C:10]3[CH2:9][C:8](=[O:19])[N:7]([C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[C:6]=2[CH:26]=1.[CH3:27][N-:28][CH3:29]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]3[CH:12]=[N:13][C:14]([C:15]([N:28]([CH3:29])[CH3:27])=[O:17])=[C:10]3[CH2:9][C:8](=[O:19])[N:7]([C:20]3[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=3)[C:6]=2[CH:26]=1

Participants

Reactant 2

HCID 182180Dimethylazanide

HCID 86735555HCID 86735555, compound

Product 1

HCID 22749551HCID 22749551, compound

Procedure

As described in previous example, 8-chloro-4,6-dihydro-6-phenyl-5-oxo-5H-imidazo[1,5-a] [1,5]benzodiazepine-3-carboxylic acid, methyl ester was converted to the dimethylamide, mp. 255°-257°.

Sources & evidence

ORD record: ord-4a1cab6a6a574430b6a34aa3ed2847d1
Source dataset: uspto-grants-1979_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04146537

Reaction notes

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