Acetic Anhydride → HCID 21327307, compound

HRID 614844Notes

Reaction equation

HRID 614844 reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[C:13]([C:15]([CH3:18])([CH3:17])[CH3:16])[CH:12]=[C:11]([NH2:19])[C:10]=1[CH3:20])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:21](OC(=O)C)(=[O:23])[CH3:22]>C1(C)C=CC=CC=1>[CH2:1]([O:8][C:9]1[CH:14]=[C:13]([C:15]([CH3:16])([CH3:17])[CH3:18])[CH:12]=[C:11]([NH:19][C:21](=[O:23])[CH3:22])[C:10]=1[CH3:20])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 21327244HCID 21327244, compound

Product 1

HCID 21327307HCID 21327307, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

This is obtained, by acetylating 2-methyl-3-amino-5-tert.-butylphenyl benzyl ether with acetic anhydride in toluene, in the form of colorless crystals; m.p. 170°-172° C.

Workup

  1. customThis is obtained

Sources & evidence

ORD record
ord-4e302ffc76da45cd8d495b61fab20dc9
Source dataset
uspto-grants-1979_03
Patent number
US04146630

Reaction notes

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