HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → 4,5-Dichloro-1H-indole-2,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 4-Chloroisatin | HCID 96047 | — |
| Product | 4,5-Dichloro-1H-indole-2,3-dione | HCID 5139980 | 70% |
Reaction Steps
Chlorination of 4-chloroisatin with sulfuryl chloride by the method of B. R. Baker, et al., J. Org. Chem., 17, 149 (1952), gave a 70% yield of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04146718 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-2e9da5e8005d4e098dd9dcb6bdeff0b7 |
| Source note | uspto-grants-1979_03 |