HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 87348375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | HCID 67305567 | HCID 67305567 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 87348375 | HCID 87348375 | — |
Reaction Steps
1.5 M of H2NOH in MeOH (0.75 ml) was added inTo a solution of methyl(1S,2S,5R)-5-[(1-acetylpiperidin-4-yl)oxy]-2-[(4-phenylpiperazin-1-yl)carbonyl]cyclohexane-carboxylate (0.1 mmol, 0.0001 mol) in 0.5 ml of MeOH. It was stirred at rt for 2 hrs. It was purified by Prep-HPLC. LCMS: (M+H)+=473.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440958B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-5b49db14aa164f5ca96142a4fbf1e743 |
| Source note | uspto-grants-2016_09 |