HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 2,3-Dihydroxypropyl 4-(n-hexadecylamino)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1,2-Dimethoxyethane | HCID 8071 | — |
| Reactant | 2,3-Epoxypropyl 4-(n-hexadecylamino)benzoate | HCID 13019377 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,3-Dihydroxypropyl 4-(n-hexadecylamino)benzoate | HCID 13019380 | — |
Reaction Steps
A mixture of 100 mg of 2,3-epoxypropyl 4-(n-hexadecylamino)benzoate, 0.2 ml of 1N sulfuric acid, and 1.0 ml of 1,2-dimethoxyethane is heated under reflux for one hour, diluted with water, and filtered to yield 2,3-dihydroxypropyl 4-(n-hexadecylamino)benzoate as a white solid, mp 112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04146546 |
| Source dataset | uspto-grants-1979_03 |
| ORD ID | ord-b06232fee77f4fc2973d22742f61c331 |
| Source note | uspto-grants-1979_03 |